Βρωμίωση της 4′-μεθυλοπροπιφαινόνης προς 2-βρωμο-4'-μεθυλοπροπιφαινόνη. Μεγάλης κλίμακας.

[Nimrod001001]

Hi friends I would like to have some of your help
I used 50g 4mp, 40ml Hbr, 15ml hydrogen peroxide 35%
this my second run after previous attempt its been to much bromine and I had green look like crystals
So I used less hydrogen peroxide
My mr stirring already for long time like 20 hours
And looks still oily and separate
Wonder why its not crystalize like in the video