Hi to All ... I Cooked Ephedrine extracted from ECA Stack Pills buyed from Nutrija an India store(Ephedrine + Caffeine + Yohimbine) ...
then I cooked it in small batch with Red Phospous+Iodine Moscow Route , and another batch with CZech route with Red phosporus Phosphoric Acid and Iodine cooked in1 hour ...
Reaction in happened but with low Yeld almost 25% ... and the final product when I do the ReCrystallization it forms Crystals But they Are long, thin, pointed and form a sort of "soft fabric" to the touch... Then I Read UNCLE FESTER 8.0 Ed book... and i found that from 2005 almost Every kind of EPhedrin Pills it's binded with a kind of High tech gum Polymers ... and he found that you could broke them only with KOH boiling it in Isopropyl Alcohol with the Ephedrine ... So I found KOH and I do This procedure ... and effectively it forms a Dark Brown Oil on the Bottom with all The Gum polymers that I have trhow away ... And I exttracted the Clear part of solution with naphta and gave me 0 purified Ephedrine ...Then I Tried with DCM and it gave me only 10 % of Yeld of Ephedrine ... UnCLE FESTER use Toluene for this passage ... Is it possible that is the only solvent that gave a Good YEld ???
I wasted almost 100 EURO pills trying to have Pure Ephedrine Crystals ... and I Have Nothing ... Could you tell me A way to obtain it ? Even ready made ... Because I have Iodine and pure red Phosporus to cook almost 10-20 Grams of Ephedrine ...
it's the only ingredient that's missing...
then I cooked it in small batch with Red Phospous+Iodine Moscow Route , and another batch with CZech route with Red phosporus Phosphoric Acid and Iodine cooked in1 hour ...
Reaction in happened but with low Yeld almost 25% ... and the final product when I do the ReCrystallization it forms Crystals But they Are long, thin, pointed and form a sort of "soft fabric" to the touch... Then I Read UNCLE FESTER 8.0 Ed book... and i found that from 2005 almost Every kind of EPhedrin Pills it's binded with a kind of High tech gum Polymers ... and he found that you could broke them only with KOH boiling it in Isopropyl Alcohol with the Ephedrine ... So I found KOH and I do This procedure ... and effectively it forms a Dark Brown Oil on the Bottom with all The Gum polymers that I have trhow away ... And I exttracted the Clear part of solution with naphta and gave me 0 purified Ephedrine ...Then I Tried with DCM and it gave me only 10 % of Yeld of Ephedrine ... UnCLE FESTER use Toluene for this passage ... Is it possible that is the only solvent that gave a Good YEld ???
I wasted almost 100 EURO pills trying to have Pure Ephedrine Crystals ... and I Have Nothing ... Could you tell me A way to obtain it ? Even ready made ... Because I have Iodine and pure red Phosporus to cook almost 10-20 Grams of Ephedrine ...
it's the only ingredient that's missing...
