ASheSChem's Amphetamine Trials and Experiments
- Thread starter ASheSChem
- Start date
Ye
Yes, that is the most probable reason for low yield from proposed pure a-oil. Question is what the dilutant was in the starting oil. A usual culprit is methanol, so in the future you could try to evaporate the oil at 50-80 C for a few hours, then steam distill the rest to purify it.
Yes, that is the most probable reason for low yield from proposed pure a-oil. Question is what the dilutant was in the starting oil. A usual culprit is methanol, so in the future you could try to evaporate the oil at 50-80 C for a few hours, then steam distill the rest to purify it.
and everything was clear after the acid-base extraction came out that the one who was making this oil diluted it with spirit ... during the water and oil evaporation and the evaporation of the dcm it started to run down with spirit. I evaporated it, I added sulfuric acid again and a beautiful clean product came out, which dried in 40 minutes.
Yes, and the spirit, from what I can read up on, is usually methanol. Up to 50% have been separated in confiscated samples of amphetamine oil.
So it makes sense to make smaller trial buys from any vendor, and then evaporate off any alcohol present in the oil. Probably steam distill it too, to get rid of any less volatile oils that can be present. Then it becomes clear just how much product one gets for every order, and finances can be calculated accordingly.
So it makes sense to make smaller trial buys from any vendor, and then evaporate off any alcohol present in the oil. Probably steam distill it too, to get rid of any less volatile oils that can be present. Then it becomes clear just how much product one gets for every order, and finances can be calculated accordingly.
I had no ingredients and I am a bit lazy, I do not want to stand so much in the kitchen, but I see that there are no other options for such times and you have to come to terms with the truth that if it is to be done well, you have to do it yourself .. ehhh
out of this smaller half, about 200g, only so much oil was saved ...
60ml oil . :/
out of this smaller half, about 200g, only so much oil was saved ...
60ml oil . :/
you can crystalize P2NP with ice water immediately this will save your much time then recrystallize with IPA or Ethanol,
I think it looks a bit sussy, did you precipitate, freeze and filter? Or just precipitation and filtration?
Looks a bit like you have left over propene in there because of the wierd crystalization, slightly yellow color.Does your product fully dissolve in water? Was your extract after basification noticeably yellow? Does it smell like your raw material?
Looks a bit like you have left over propene in there because of the wierd crystalization, slightly yellow color.Does your product fully dissolve in water? Was your extract after basification noticeably yellow? Does it smell like your raw material?