3-(1-Naphthoyl)indole Synthesis
- Thread starter WillD
- Start date
as we talked on private, remove insoluble when add water with ice. and then add ethyl acetate.
first time I not remove insoluble and get sticky stuff, next time I filter out and remove insoluble and add ethyl acetate and get the product like it should be.
first time I not remove insoluble and get sticky stuff, next time I filter out and remove insoluble and add ethyl acetate and get the product like it should be.
actually. if you get naphtoyl indole in sticky gum form and cant evaporate last bits of EA, what really works is this.
You put all that sticky oil naphtoyl indole into water and stirr for few minutes. It gets all trapped EA out of naphtoyl indole then you filter and put to dry.
After added tail, compound very active.
You put all that sticky oil naphtoyl indole into water and stirr for few minutes. It gets all trapped EA out of naphtoyl indole then you filter and put to dry.
After added tail, compound very active.
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Hello everyone... Please, I find it difficult to obtain Tin(IV) chloride, and I found that its synthesis is also difficult. I have Tin(II) chloride, so is it possible to use it? Are there other alternatives that can be used instead?
