Aluminium amalgam (Al/Hg) Summary
Ali je to mogoče uporabiti za nadomestitev sintez, pri katerih je potreben NaBH4? Poskušam izdelati 5-MeO-DMT iz 5-MeO-T po sintezi Hamiltona Norrisa, vendar nimam na voljo NaBH4.
- By G.Patton
Mislim, da ne
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ali obstaja način za izdelavo NaBH4, ki ne zahteva super visokih temperatur ali tlaka in ga je mogoče narediti v majhnem obsegu v amaterskem laboratoriju, ali naj se kar vdam in naročim na Kitajskem ter upam, da me carina ne bo zaslišala?
Zakaj Al/Hg ne deluje za to sintezo: moral bi reducirati imin, da bi metiliral triptamin, ne?
Mislim, da bi bilo to mogoče, vendar nisem popolnoma prepričan. Ali menite, da se bo zmanjšala dvojna vez na indolu?
Edina stvar, o kateri nisem preveč prepričan, je izdelek, ali bo izdeloval MMT ali DMT. Pri vaši sintezi metamfetamina iz amfetamina z Al/Hg se aminu doda le ena metilna skupina.
Kako po pripravi raztopine živega srebra v dušikovi kislini, ki jo nato dodamo v bučko z vodo in aluminijasto folijo, pravilno odzračiti hlape te reakcije? Zdi se, da so hlapi dovolj močni, da uhajajo iz zračnega filtra in gredo tudi skozi masko. Razmišljal sem, da bi uporabil vakuumsko črpalko z erlenmajerico in nato regulator vakuuma, tako da bi bil vakuum dovolj močan, da bi se hlapi odvajali ven, vendar me skrbi črpanje vodikovega plina, saj bi lahko prišlo do eksplozije.
Pozdravljeni, ali lahko za sintezo amfetamina uporabim enako količino živosrebrovega (Ii) klorida kot živosrebrovega (Ii) nitrata, pls
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
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A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol
