Эфедрон из гидрохлорида эфедрина

DHHood

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Mit kaliumpermanganat funktioniert es auch, man muss nur exakt messen, genau timen und wissen wie giftige beiprodukte, sofern entstanden, zu entfernen sind. Dazu ist mehr als chemisches Grundwissen gefragt, obwohl die Synthese so simpel ist dass sie jeder durchführen kann.

Ich habe abzugeben :
* Chrome(III)oxide
* Kaliumpermanganate
* Ephedra sinica from China (2.5-5% ephedrine type alkaloids with l-ephedrine being the most with 90%
* I can offer extraction of ephedrine from the herb and deliver clear white ephedrine hcl extract which is of very high purity and can directly be used for further synths
* almost pure pseudoephedrine Extracted from pills and seperated from the ibuprofen also present in its pill form
... also i have 3-4g ephedrone methcathinone (made with l-eph&kmno4) to give away, maybe one would to thank by Sending a few Euros 4 IT. Should be basified and washed with Walter to remove excess salt which is in product.

Best regards
D

....

All chemicals Like acids (phosphoric, hcl, sulphur ect) , bases, oxidizing agents, iodine / Jod, alcohols like Ethanol, Methanol, Loesungs-/Reinigungsmittel dmso, Aceton, dcm methylene Chlorid, ether, terpentine, naphta, ipa, heptane and EVERY other can be offered by me, Text me if u need a quotation...
 

KensonKen

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Dear DHHood - we look for a new vendor for Ephedrine Powder? Can you sell it?
 

YenaneY

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Okay, but why will H2O2 not work? Or more generally no other oxidizer than kmno4 or Chrome oxidizer?
 
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DHHood

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Because u need an agent which oxidizes secondary alcohols to ketones, u cant just take anyone..... Also h2o2 is needed for the synth IT is Not an oxidizing agent, the ones u need are chromes in the +6 State f.e. chrome(VI) oxide, sodium/potassium/Ammonium dichromate ect... Look up Jones reagent for more Info
 

YenaneY

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Okay thx, I oversaw that...
But regarding oxidizing agents that oxidize specifically secondary alcohols to ketones, I read sodium hypochlorite does?
Also i'm interested in you offer, I'll write dm
 

DHHood

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IT May work with sodium hypo., i dont know..... But why Do that?

With chrome(VI)oxide u get a clean and pure product and this synthesis is the Status quovquo w detailed manuals, also will be finished in a couple hours...

Kmno4 works too, but will take over night and u have to watch out for manganese which is a byproduct and Really dangerous.
 

Eleusius_hive_reboot

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PLEASE BELIEVE ME, HYDROGEN-PRROXIDE (3%) F. DRUGSTORE DOES THE JOB IN ACETIC ACID !

QUENCH WITH SODIUM-BISULFITE AND BOOM1 DONE

KmnO4 LEAVES TRACE AMOUNTS OF TOXIC BRAIN DAMAGING COMPOUNDS 1 VERY TRICKY TO GET IT OUT COMPLETELY, NOT A GOOD WORKUP...
 
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