Mefedrona (4MMC) kristalizācija

rado

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Sveiki visi!

Kā es varu kristalizēt gatavu mef ūdens šķīdumu, izmantojot NaCl, ja man sākotnēji nebija miltu? Teiksim, man ir mef bāze dihlormetānā, un es to paskābināšu ar pārlieku lielu ūdens daudzumu 135 ml uz 100 mef, vienlaikus izšķīdinot mef ūdenī - es neievietoju mef miltos, bet uzreiz ūdenī.

Kādā posmā pievienot NaCl un kādās proporcijās. Saskaņā ar augšējo pieredzi autors norāda 23 gramus uz 100 gramiem mef, bet viņam ir 100 gramu mef, kas izšķīdināti 100 ml ūdens. Un mana oksidēšanās notiek ar 135 ml uz 100 g produkta.

Cik ilgi veidojas kristāli, izmantojot NaCl sāls šķīduma metodi? Kāda lieluma frakcijas tiek iegūtas? cik ilgi produkts jāglabā saldētavā? Vai iedarbības laiks ietekmē kristāla lielumu?

Paldies visiem!
 

PolandoEmingarnte

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uz dcm tā nevar darīt, paskābināšanas procesā ir jāizmanto ūdens un pēc tam jāizmanto, piemēram, ipa, lai nekavējoties sāktu kristalizācijas procesu. Naci vispār nav vajadzīgs, tā ir muļķība. un jūs nevarat sasaldēt, jo kristāls neiznāks tikai stikla un kristāla pulvera veidā.
 
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mcdonalds

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amigo,
quieres decir que en la reaccion entre la bromoketona y la metilamina utilizas dmso en lugar de Diclorometano?
 

Savitar

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Brine cristalisation grom yesterday - everything happen in about one hour. But its recrystalisation of 3cmc. At the same time i maked 3 other kind of crystalisation. The biggest crystal (yes one big crystal) is in only vodka. The most beautifull is on 1 ml dh2o/1g powder, boiled few minutes in atomic generator 🤣 and later i used only ceramic lamp
DztAlRVKyO
SgIr2jOhmx
 

UltraHQ

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Can you show the one big crystal that you mention?
 
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Savitar

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I have only after crashing and washing in progress...
GE0tZWRQrh
 

UltraHQ

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Oh nice, if you break it up more it will help you remove the colouration of the crystal otherwise the acetone won't be able to penetrate the solid mass of that crystal. You could probably get that white if it was broken down more.
 

TheVacuumGuy

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My latest crystal, from a failed batch which i put in a beaker and used as container to drip remainders of solvents, acids andsoforth. After some weeks i needed the beaker and while cleaning it, i found these.

Now i want to make these on purpose but how... without using loads of beakers as a waste bin :ROFLMAO:



LrQ9zp3AcS
 

Yogi

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TheVacuumGuy

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I haven't thought of that. Gonna try it straight away 🤭😑
 
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