Aluminium amalgam (Al/Hg) Summary
Kas seda saab kasutada NaBH4-d nõudvate sünteeside asendamiseks? Püüan teha 5-MeO-DMT-d 5-MeO-T-st Hamilton Norrise sünteesi järgi, kuid mul ei ole NaBH4-i kasutada.
- By G.Patton
Ma ei usu, et
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kas on olemas viis NaBH4 valmistamiseks, mis ei nõua ülikõrgeid temperatuure või rõhku ja mida saab teha väikeses mahus amatöörlaboris, või annan lihtsalt alla ja tellin Hiinast ja loodan, et toll ei sea mind kahtluse alla?
Miks ei tööta Al/Hg selle sünteesi puhul? see peaks vähendama imiini, et metüleerida trüptamiini, mitte?
Ma arvan, et see võib olla võimalik, kuid ma ei ole täiesti kindel. Kas te arvate, et see vähendab indooli kaksiksidet?
Üks asi, milles ma ei ole liiga kindel, on toode, kas see teeb MMT või DMT. Teie metamfetamiini sünteesis amfetamiinist Al/Hg-ga lisatakse amiinile ainult üks metüülrühm.
Pärast elavhõbeda lahuse valmistamist lämmastikhappes, seejärel selle lahuse lisamist kolbi koos vee ja alumiiniumfooliumiga, kuidas saab selle reaktsiooni käigus tekkivad aurud õigesti õhku lasta? Aurud tunduvad olevat piisavalt tugevad, et need väljuvad õhufiltrist ja lähevad ka läbi maski. Ma mõtlesin kasutada vaakumpumpa koos kolbiga ja seejärel vaakumregulaatorit, nii et vaakumi tugevus on just piisav, et aurud saaks väljapumbata, kuid ma olen mures vesinikgaasi pumpamise pärast, kuna see võib põhjustada plahvatusohtu.
Tere, kas ma saan kasutada sama koguse elavhõbe(Ii)kloriidi nagu elavhõbe(Ii)nitraati amfetamiini sünteesiks pls
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
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A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol
