Aluminium amalgam (Al/Hg) Summary
¿Se puede utilizar para sustituir síntesis que requieran NaBH4? Estoy intentando hacer 5-MeO-DMT a partir de 5-MeO-T siguiendo la síntesis de Hamilton Norris, pero no dispongo de NaBH4.
- By G.Patton
No lo creo
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¿hay alguna manera de fabricar NaBH4 que no requiera temperaturas o presiones superaltas y que se pueda hacer a pequeña escala en un laboratorio de aficionado, o simplemente me rindo y hago un pedido a China y espero que la aduana no me interrogue?
¿Por qué no funciona el Al/Hg para esa síntesis? debería reducir la imina para metilar la triptamina, ¿no?
Creo que puede ser posible, pero no estoy totalmente seguro. ¿Cree que reducirá el doble enlace del indol?
Lo único de lo que no estoy muy seguro es del producto, si hará MMT o DMT. En tu síntesis de metanfetamina a partir de anfetamina con Al/Hg, sólo se añade un grupo metilo a la amina.
Después de preparar una solución de mercurio en ácido nítrico y añadirla a un matraz con agua y papel de aluminio, ¿cómo se ventilan correctamente los humos de esta reacción? Los vapores parecen tan fuertes que se escapan del filtro de aire y atraviesan también la mascarilla. Estaba pensando en utilizar la bomba de vacío con el matraz y luego un regulador de vacío para que la fuerza del vacío sea suficiente para que los humos se ventilen al exterior, pero me preocupa el bombeo de gas hidrógeno, ya que podría correr el riesgo de explosión.
Hola, ¿puedo utilizar la misma cantidad de cloruro de mercurio (Ii) que de nitrato de mercurio (Ii) para sintetizar anfetamina?
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
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A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol
