MDMA synthesis via NaBH4 from MDP2P

[AKWA]

Anhydrous. Or as close to

 

[Studenttt]

When i have the mdma freebase i mix it 1:2 white aceton and bring ph to 2/3 and put it in freezer for 24 hours.
But nothing come? Somebody can help me?

 

[Jordan Belfort]

Did you try the freebase probably reaction wasn't successful

 

[PolandoEmingarnte]

u say u made 500kg mdma now u cant made ?? xd

 

[Woodshack]

Your Ratios are all wrong, You need a ph range of 7 - 6.5, because your PH is 2-3 your powder will solute again. Your next problem is that you need to make sure your Acetone is anhydrous and you need a Freebase to Acetone ratio of 1:4.

 

[Jordan Belfort]

Depends how cold your freezer goes

 

[Mr Good Cat]

I guess you overestimate MDMA FB solubility in DCM, petroleum ether, hexanne and similar solvents. In the reality it is about 3-4 ml of those solvents per 1 gr of base.

 

[Jordan Belfort]

Do you also known for meth base ?

 

[Mr Good Cat]

Nop. This MDMA data it got empirically.

 

[Mr Good Cat]

Funny, but MDP2P cas 4676-39-5 and NaBH4 here are used in molar proportions 5.78 (1000 gr) : 2.56 (100 gr). Is it a mistake?

 

[G.Patton]

No, it isn't. It is a necessary excess.

 

[Mr Good Cat]

@G.Patton general, is there any advantage to use Methylamine aqueous solution cas 74-89-5 against Methylamine HCl cas 593-51-1 + NaOH?

 

[G.Patton]

There is no an option to use methylamine water solution with NaBH4.

 

[Mr Good Cat]

If I understand it correctly, T must be kept 8-10C while all the stirring process.

What is expected ice consumption for 20-30L jacketed reactor used with a pump, submerged to a ice bath? Or this is wrong concept, and better to target for flow electric cooler?

 

[G.Patton]

during NaBH4 addition, you can stir at room temp for 2 days.
Hi, I can't answer you. Depends on your addition speed and other factors.

 

[alquimista00]

sodium boronhudridecanbe substituted for something different in this process that perfoms the same function.

 

[Win Win]

Can change methylamine hci to solution?

 

[G.Patton]

I don't understand your question.

 

[Win Win]

Your method is using methylamine gas right? But methylamine is use methylamine HCI mix with methanol right? Can use methylamine solution to replace methylamine HCI?

 

[G.Patton]

Do you understand that methylamine gas is used in order to make methylamine methanol (MeOH) solution? Not methylamine hydrochloride methanol solution. You can directly use methylamine free base methanol solution.

 

[Win Win]

Noted with thanks

 

[2-79-790125]

I had the same question. I have a stockpile of methylamine HCl . wondering how to use that correctly with this process.....