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P2NP

Letswork2025

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Is there any other methods of getting P2np ? nitroethane is highly watched where I am ? Or would p2p be a better option for me ? I’m only needing to do small amounts at a time
 

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Try to obtain propionic esters if you can they are easier to come by and are cheaper than nitroethane then by darzens reaction you get glycidic esters upon hydrolysis you get P2P.

If not P2np, P2P should do the job with some extra work.

Clearnet:

 

Dr. MMX

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Nitroethane is a solvent used widely in the some of the industries, some special " cleaners" for ink printers do contain it for example.
P2NP is far more "weird" than nitroethane, p2p has only obvious purpose :)
 

HIGGS BOSSON

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Unfortunately, p2np cannot be obtained without nitroethane, so in its absence it is necessary to consider the routes of p2p synthesis, of which there are many more.
 

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There is 2-nitropropene which can be used in the synthesis and isnt as watched as nitroethane, and then FE/HCL/Fecl3, SnCl2/HCL, zn/hcl, and there is a option to stop at the oxime stage, remove hard particalse, neutralize acid, and extract and re-crystalize oxime for better purity.
 

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Iv chosen to attempt to obtain p2p instead as I’m a beginner and that route seems more simple for me and the ingredients are more easy to obtain. Once iv got the p2p can I use one flask for steam distillation? I only have a 1000ml flask a condenser and a 250ml receiver. I don’t have an extra flask to act as a steamer ? Can I add more water to the 1000ml and use just the one flask? Hope that makes sense
 

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Look now, prepare the more clean SnCl2 reduction of p2np, then get the ketone in non-polar, remove the nonpolar, and vacum/steam destill the p2p.
 
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