Syntese af 5-MeO-DMT fra 5-MeO-Tryptamin

[MadHatter]

Hamilton Morris gør dette på Youtube:

Det laboratorium, han arbejder i, er ægte laboratorieporno. Fungerer som illustration til denne fremragende artikel!

 

[mycelium]

Thanks, hatter

 

[tripeep]

Hvor mange milliliter 37 % formaldehydopløsning skal der bruges?

 

[G.Patton]

Brug venligst engelsk sprog i fælles afsnit.

 

[tripeep]

Hvor mange ml 37 % formaldehydopløsning er der brug for?

 

[G.Patton]

Hej, ækvimolar mængde 26,25 mmol (som 5-MeO-Tryptamin). Tæl det i 37% aq opløsning.

 

[tripeep]

Kan natriumborhydrid erstattes med kaliumborhydrid med samme antal mmol?

 

[mycelium]

It says a solution of 37% formaldehyde stabilized w 12% meoh , which I assume to be an 88% formalin and 12% meoh, an I correct? Or would it be 100% formalin and 12% MeOH?

 

[bigdigrandy]

Ville en reduktion med natriumhydrid også fungere, fordi NaBH4 er reguleret, hvor jeg bor, men jeg har fundet en pålidelig leverandør af NaH

 

[tripeep]

Kan natriumborhydrid erstattes med kaliumborhydrid med samme antal mmol?

 

[G.Patton]

Hallo, ja.

 

[Swirly]

Here is a guide for this reaction:

Synthesis of 5-MeO-DMT from 5-MeO-Tryptamine : SwirlyBird : Free Download, Borrow, and Streaming : Internet Archive

Detail of a Chemistry Eperiment

archive.org

or

https://archivep75mbjunhxc6x4j5mwjmomyxb573v42baldlqu56ruil2oiad.onion/details/5-me-odmtsynthy

Again, try and use paraformaldehyde dissolved in methanol with the help of Sodium metal.

 

[mycelium]

Wow, that is amazing.
I have lots of experience with dry ice baths, and lots of experience with throwing scoops of DI into the alcohol in the condenser , and it just exploding into the lab...dry ice and IPA.. ALCOHOL(OR ACETONE) into the dry ice works a lot better.
And hearing the stainless squeak and sound like it is ripping apart, just from the temp change ..