- Language
- 🇨🇿
- Joined
- Feb 12, 2022
- Messages
- 91
- Reaction score
- 94
- Points
- 18
4,8g PseudoE
2,5g RP
6g I2
1,5ml H3PO4
oil bath
4 Hours Reflux
after reaction:
150ml DH2O
add NaOH PH 12+
100ml Xylene
wash with warm, cold DH2O
separate funnel
+20ml DH2O
+20ml DH2O
add 35%HCL PH 7
evaporate in heat
washed with cold Acetone
recrystalization in Isopropylalcohol with acetone
left in the freezer for 12 hours
filtered
2,5g RP
6g I2
1,5ml H3PO4
oil bath
4 Hours Reflux
after reaction:
150ml DH2O
add NaOH PH 12+
100ml Xylene
wash with warm, cold DH2O
separate funnel
+20ml DH2O
+20ml DH2O
add 35%HCL PH 7
evaporate in heat
washed with cold Acetone
recrystalization in Isopropylalcohol with acetone
left in the freezer for 12 hours
filtered
Attachments
-
XJswKGMT5C.jpg1.4 MB · Views: 475
-
h6NTuMU9c1.jpg1.4 MB · Views: 402
-
AoBEpviq6s.jpg1.4 MB · Views: 402
-
wcmBvEnA4k.jpg1 MB · Views: 407
-
2yvJkLaSHj.jpg1.7 MB · Views: 398
-
V7CgynN6zT.jpg1.2 MB · Views: 420
-
R92LqAJQPy.jpg956.9 KB · Views: 415
-
kbuSEiX5y9.jpg1.3 MB · Views: 425
-
idVobEk7If.jpg992.9 KB · Views: 401
-
kCYHLs0enK.jpg976.2 KB · Views: 381
-
pwtzxRqfnO.jpg3 MB · Views: 408
-
fhjSBtEpuK.jpg1,021.8 KB · Views: 400
-
ZDlSX8JICA.jpg976.6 KB · Views: 371
-
uPUnhYj2Lv.jpg3.7 MB · Views: 411
-
tZJ7pqXHy4.jpg1.1 MB · Views: 390
-
cEz8puGhKy.jpg1,013.2 KB · Views: 389
-
d6k7xp8ZDh.jpg800 KB · Views: 378
-
PDwZmgzcB3.jpg1 MB · Views: 375
-
pFEbv91fc3.jpg1.3 MB · Views: 414
-
lQxwqtUAbJ.jpg1.1 MB · Views: 400
-
sPqpUCg0lc.jpg804 KB · Views: 402
-
OFkr1tYRE9.jpg1.2 MB · Views: 433
-
UpXZjaf12N.jpg810 KB · Views: 418
-
GQJauexbD4.jpg1.2 MB · Views: 464
Last edited: