Extraction of Amides from Lysergic Acid: Start with Morning Glory national seeds, the young seeds of the Hawaiian wooden baby Rose, ergot cultured or naturally ergot compounds occurring.
NOTE: Morning glory seeds can be coated with a toxic chemical by the seed company in order to avoid ingestion. If a package of seeds contain coated seeds this fact shall be stated in the container. Soaking the seeds in hot water for 1/2 hour and Rinsing on a filter should remove this coating. while many varieties of morning glory contain the active LSA (Lysergic acid amide), the yield varies greatly. Therefore, the use Pearly only gates, Wedding Bells, and Sky Blue varieties for The best results.
Reduce the seed material to a fine powder in the blender, and spread it to dry. Grind again if not good enough after the first time due to humidity.
Saturate powdered seed material with lighter fluid, naphtha, or Ligroin.
When completely saturated, it should have the soup consistency. Pour into a chromatographic column and let sit overnight.
Remove the fatty oils from the material by drip to solvent slowly through the column, and testing the liquid that comes through fats by evaporation of a drop in clean glass until it doesn't leave greasy film. (Must have several grams of solvent for each gram of seeds).
Mix 9 volumes of chloroform with 1 volume of concentrate ammonium hydroxide and stirring in a separation funnel. When settling, the chloroform phase will be at the bottom. Drain the chloroform layer and discard the top layer.
Drip the chloroform wash through the column and save the extract. continuously test by evaporation of a drop in cleaning glass until it stops fluorescence.
It is not explicit in the source, but if it is extracted From ergot I would like to start with the alkaloid base of Cravage in this point
The chloroform extracts evaporate, and dissolve the residue in the minimum amount of a 3% solution of tartaric acid. If all the residue does not dissolve, put it in suspension by agitation forcefully.
Colour of the solution with an acid-base indicator, and titre of Find the approximate number of moles of the present alkaloid.
Transfer the solution to a settling funnel, and wash the another ship with acid in order to get all the alkaloids out. Pour the washing liquid into the funnel as well.
Bring the pH to make the solution basic by adding sodium a solution of bicarbonate, and add an equal volume of chloroform.
Shake well, let it resolve, remove the background layer and Book. Again add an equal portion of chloroform, shake, let's solve and remove bottom layer.
Combine chloroform extracts (bottom layer) and it evaporates.
The residue remaining after evaporation is a semi-pure LSA concentrate (lysergic acid amide). Amide requires some experimentation for dosage, but 1 mg of the concentrate It's a reasonable starting point. 1 mg LSA will produce effects comparable to 100 micrograms of LSD.
If there's anything wrong, please correct me, using the translator is bad.
NOTE: Morning glory seeds can be coated with a toxic chemical by the seed company in order to avoid ingestion. If a package of seeds contain coated seeds this fact shall be stated in the container. Soaking the seeds in hot water for 1/2 hour and Rinsing on a filter should remove this coating. while many varieties of morning glory contain the active LSA (Lysergic acid amide), the yield varies greatly. Therefore, the use Pearly only gates, Wedding Bells, and Sky Blue varieties for The best results.
Reduce the seed material to a fine powder in the blender, and spread it to dry. Grind again if not good enough after the first time due to humidity.
Saturate powdered seed material with lighter fluid, naphtha, or Ligroin.
When completely saturated, it should have the soup consistency. Pour into a chromatographic column and let sit overnight.
Remove the fatty oils from the material by drip to solvent slowly through the column, and testing the liquid that comes through fats by evaporation of a drop in clean glass until it doesn't leave greasy film. (Must have several grams of solvent for each gram of seeds).
Mix 9 volumes of chloroform with 1 volume of concentrate ammonium hydroxide and stirring in a separation funnel. When settling, the chloroform phase will be at the bottom. Drain the chloroform layer and discard the top layer.
Drip the chloroform wash through the column and save the extract. continuously test by evaporation of a drop in cleaning glass until it stops fluorescence.
It is not explicit in the source, but if it is extracted From ergot I would like to start with the alkaloid base of Cravage in this point
The chloroform extracts evaporate, and dissolve the residue in the minimum amount of a 3% solution of tartaric acid. If all the residue does not dissolve, put it in suspension by agitation forcefully.
Colour of the solution with an acid-base indicator, and titre of Find the approximate number of moles of the present alkaloid.
Transfer the solution to a settling funnel, and wash the another ship with acid in order to get all the alkaloids out. Pour the washing liquid into the funnel as well.
Bring the pH to make the solution basic by adding sodium a solution of bicarbonate, and add an equal volume of chloroform.
Shake well, let it resolve, remove the background layer and Book. Again add an equal portion of chloroform, shake, let's solve and remove bottom layer.
Combine chloroform extracts (bottom layer) and it evaporates.
The residue remaining after evaporation is a semi-pure LSA concentrate (lysergic acid amide). Amide requires some experimentation for dosage, but 1 mg of the concentrate It's a reasonable starting point. 1 mg LSA will produce effects comparable to 100 micrograms of LSD.
If there's anything wrong, please correct me, using the translator is bad.
