Hi everyone !
I need you to a recipe that i don't know.
Usually, to get amph sulphate from a-oil, I used sulfuric acid + aceton, as explain here : http://bbzzzsvqcrqtki6umym6itiixfhn...mine-synthesis-from-p2np-via-al-hg-video.196/
But not long ago, I was invited to see an another way.
To do it, we used :
- 2 000 mL of A-oil
- 3 060 mL of Methanol
- 440 g of Sulfuric acid 98%
My role was only to listen and do what we asked to me (not to interfer during the process).
How it happened :
- First of all, we put all ingredient into freezer to have smoother reaction later with sulfuric acid.
- Then we mixed Oil with Methanol.
- Around 10-15min later, to be sure that the solution was very good mixed, we had slowly acid and continued to mixed.
- At the end, PH was 7.8. We put it in freezer for 20 hours.
- Because of small freezer, final mixture was cut in 4 parts in it. Between the end of mixing and moment when we put last part in the fridge, PH has upgraded to 8.1.
- With 2 L amph base, we make around 4,5kg.
I was very disappointed after that because many question came, but people who show me that are not chemist, just follow a recipe they have...
So first of all, do you know if it's a legit ways to make amphetamine sulfate from a-oil ?
We doesn't make any filtration, some residual solvent can be still present and bring down purity ?
Ph 7,8 is it enough ? The way that it go back to 8.1 is it a problem ?
Final result was white past, but locally we can see yellow/orange spot ( very localize and not seems to expand).
May be you need more info that I forbidden to say, just notice me
and if this case was already on an other post, i really apologize for the inconvenient !
Thanks to all of the you !
I need you to a recipe that i don't know.
Usually, to get amph sulphate from a-oil, I used sulfuric acid + aceton, as explain here : http://bbzzzsvqcrqtki6umym6itiixfhn...mine-synthesis-from-p2np-via-al-hg-video.196/
But not long ago, I was invited to see an another way.
To do it, we used :
- 2 000 mL of A-oil
- 3 060 mL of Methanol
- 440 g of Sulfuric acid 98%
My role was only to listen and do what we asked to me (not to interfer during the process).
How it happened :
- First of all, we put all ingredient into freezer to have smoother reaction later with sulfuric acid.
- Then we mixed Oil with Methanol.
- Around 10-15min later, to be sure that the solution was very good mixed, we had slowly acid and continued to mixed.
- At the end, PH was 7.8. We put it in freezer for 20 hours.
- Because of small freezer, final mixture was cut in 4 parts in it. Between the end of mixing and moment when we put last part in the fridge, PH has upgraded to 8.1.
- With 2 L amph base, we make around 4,5kg.
I was very disappointed after that because many question came, but people who show me that are not chemist, just follow a recipe they have...
So first of all, do you know if it's a legit ways to make amphetamine sulfate from a-oil ?
We doesn't make any filtration, some residual solvent can be still present and bring down purity ?
Ph 7,8 is it enough ? The way that it go back to 8.1 is it a problem ?
Final result was white past, but locally we can see yellow/orange spot ( very localize and not seems to expand).
May be you need more info that I forbidden to say, just notice me
and if this case was already on an other post, i really apologize for the inconvenient !
Thanks to all of the you !
