4’mmc in dcm helppp

[Sig]

Hello gays I have bk4 in dcm
15 liter like this i do to fast methylamine end I go over the boiling point now is dirty can I clean it ..

Second when I put freebase dcm
Water and acid ph 5 upper layer is green ??

is it possible to make freebase directly to. Cristals in Freeze ?? Like mdma..

 

[Sig]

Freebase in dcm I do to fast mythylamine and it go boiling I think to dirty now

 

[antrax]

In my case I add 5l of DCM for every 1kg of precursor, but you can add the necessary amount of DCM until the precursor is correctly dissolved and throughout the process you must stir it....
Then you must add the 40% methylamine solution to the dissolved precursor, I add 2l of 40% methylamine aqueous solution for every 1kg of precursor, less quantity may be fine, and it is better to add the 40% methylamine aqueous solution little by little, small amounts every 5-10 minutes, because if you add everything at once the dissolved precursor can overheat and the synthesis fail, you must stir at all times....

 

[Sig]

I do to fast it’s it’s overhead next time better

 

[antrax]

How is it possible that you have 15 liters in DCM? how much precursor have you used

 

[Sig]

i have 50 liter reactor I put 5 kg 2b4m 15 liters dcm and 10l amine i do first 20 degrees dcm and put bk4
after I do the methyl amine to. fast and go to 40/41 hey boiling same time.

 

[Sig]

Second batch I do only 1 kg and easy white te mythylamine 1,5 uhr I think go great only 32 degrees but in the last 30 min the collor change to darker

 

[Sig]

Today I make a small to powder no succes I need wash a couple
Times to get it wite

 

[antrax]

you failed the synthesis, there's no way to go back, just throw that away

 

[Sig]

I clean clean clean now cristals comes

 

[antrax]

What chemical have you washed it with and with what quantities?

 

[Sig]

Quantities I see at the end

 

[Sig]

I dont look how match? I look collor.
4 times I think I need with acetone

 

[antrax]

but u do it for fun or for making profit, because if u do it for making mony u need to know all quantities....