mephedrone ethyl acetate synthesis

  1. Toddler

    I trying 4mmc?

    plz check the whole process and plz tell me which step i do mistake, mixture not perform white Flappy liquid. 20g 2b4m 100ml EA stirrer until dissolve, Then add 40ml MA 40%. stirrer 1 hours temp not goes above 30.2. Without water bath. then put in separating funnel. first wash once with...
  2. William D.

    Mephedrone (4-MMC) synthesis from haloketone in ethyl acetate. 1-10 kg Scale.

    Reaction scheme: Reagents: 1. 4'-Methylpropiophenone (cas 5337-93-9) 1 kg; 2. Hydrobromic acid 48% 1300 ml; 3. Hydrogen peroxide 35% 750 ml; 4. Sodium/potassium hydroxide 25% (NaOH/KOH) aqueous solution; 5. Distilled water; 6. Ethyl acetate 6 l; 7. Methylamine 40% aq - 2 l; 8. Acetone - 8 l...
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