mcat

plz check the whole process and plz tell me which step i do mistake, mixture not perform white Flappy liquid. 20g 2b4m 100ml EA stirrer until dissolve, Then add 40ml MA 40%. stirrer 1 hours temp not goes above 30.2. Without water bath. then put in separating funnel. first wash once with...

So i first added 2b4mp then bezen in flask then i added methylamine 40% and started stiring with megnetic stirrer, now i don't have heat source so how long should i stirrer for without heat? And how will i know the reaction is done? At starting the liquid was white right now its turned greenish...