2-bromo-4-methylpropiophenone 1451-82-7 bk4 2b4m
CAS:1451-82-7
White crystals
Purity:99%
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plz check the whole process and plz tell me which step i do mistake, mixture not perform white Flappy liquid.
20g 2b4m
100ml EA
stirrer until dissolve,
Then add 40ml MA 40%.
stirrer 1 hours temp not goes above 30.2. Without water bath.
then put in separating funnel.
first wash once with...
So in my attempts finding a a supplier for some 2B3M (CAS : 1451-83-8), i've made some inquiries.
The inquiries cam down to :
CAS : 1451-83-8
Amount: 10kg, (repeated at some interval, when satisfied).
Incoterm: the least hassle, so think DDP or (DPU which i didnt know existed)
overview of...
You can scale it proportionally (in large amounts methylamine may be added in more parts)
Reagents:
1. 2b4m 100g;
2. Ethyl Acetate 500ml;
3. Distilled water ~2l;
4. NaOH 100g;
5. Methylamine HCL 150g;
6. Acetone 500-1000ml;
7. HCL acid 50-70 ml;
Equipment:
1. Magnetic stirrer;
2. Beaker 200ml...
I was looking over the properties of Hexane, and it seems a good fit do use as solvent .
It is also cheap. Anyone experience with it for Mephedrone synthesis ?