1-naphthoyl chloride
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JWH-018 synthesis
Reaction scheme: Equipment and glassware: 50 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system (cooling) and reflux condenser; 10 L Flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Top stirrer; Heating...- WillD
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- 1-naphthoyl chloride 1-pentyl-3-(1-naphthoyl)indole 3-(1-naphthoyl)indole synthesis am-678 cannabinoid synthesis cas 109555-87-5 cas 209414-07-3 jwh synthesis jwh-018 jwh-018 synthesis
- Replies: 174
- Forum: Cannabinoids
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3-(1-Naphthoyl)indole Synthesis
Reagents: Indole (cas 120-72-9) 1000 g; Dichloromethane (CH2Cl2) 15 l; Tin(IV) chloride (SnCl4) 2000 ml; 1-Naphthoyl chloride (cas 879-18-5) 1627 g; Nitromethane (cas 75-52-5) 10 l; Distilled water 20 l; Ethyl acetate (EtOAc) 15 l; Sodium or magnesium sulphate (Na2SO4 or MgSO4); Equipment and...- WillD
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- 1-naphthoyl chloride 3-(1-naphthoyl)indole synthesis cas 109555-87-5 cas 879-18-5 indole jwh 018 jwh-018
- Replies: 35
- Forum: Cannabinoids
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JWH-018 synthesis. Small scale.
Reaction scheme: Reagents: Indole (cas 120-72-9) 0.117 g; Aluminum oxide (Al2O3) 1 g; 1-Naphthoyl chloride (cas 879-18-5) 0.286 g; Sodium carbonate (Na2CO3) 0.16 g; 1-Bromopentane (cas 110-53-2) 0.18 g; Ethanol (EtOH) 60 ml; Distilled water; Equipment and glassware: Microwave vial 5 ml...- WillD
- Thread
- 1-naphthoyl chloride cannabinoid cas 110-53-2 cas 120-72-9 cas 209414-07-3 cas 879-18-5 jwh-018 microwave synthesis jwh-018 small scale jwh-018 synthesis spice
- Replies: 91
- Forum: Cannabinoids