Jednoduchá surová syntéza Δ8-THC bez rozpúšťadiel, otázky

cvvvxa

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Dobrý deň, narazil som na to na youtube a chcel som sa podeliť a opýtať sa, či s tým má niekto nejaké skúsenosti, prípadne zlepšováky, keďže plánujem robiť vo veľkom. Angličtina nie je môj materinský jazyk, takže sa ospravedlňujem za chyby
zdroj :

Postup:
CBD (25g) sa zmieša s P-TSA (0,5g) a umiestni sa na varnú dosku nastavenú na 120C, mieša sa a zahrieva sa hodinu. Potom zmes obsahuje 75% Delta 8 THC, 2,5% Delta 9 THC, 4% CBDA, 5% exo-THC, 10% izo-THC.

Moja hlavná otázka je, či by sa to dalo fajčiť po zmytí kyseliny vodou a zásadou a či by sa Δ9 dalo vyrobiť možno zahriatím na 70C a dlhším udržaním. Už som videl metódy na výrobu Δ9, ale s rozpúšťadlami, a tomu sa chcem vyhnúť, pretože v porovnaní s týmto je to otrava zbaviť sa litrov toluénu. Tiež či by bolo možné odstrániť červenú farbu.
 

WillD

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Je potrebné používať rozpúšťadlá. A ďalšie podmienky s týmto činidlom
 

mycelium

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There is a whole website devoted to cannabis extraction, which also includes a grip of CBD>D8 or d9.
PTSA is one way, I believe there is also a catalyst required.
I haven't been doing canna work for a few years and never did those reactions, but there are several paths that use different chemicals some make a lot of d8, some make a lot of d9, but ZERO people , and these are weed chemists a lot of them, have make d8 that does not have d9, and chromotography won't seperated them(what I read was a lot of solvent to seperated and the cost is crazy.

The d9 conversion is just as potent as distillate from weed, but it has a dif flavor(not that distillate has flavor, but yeah)
 

mycelium

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Further more, unless you have a grip of solventless CBD, then I don't know what you would start with solventless, because you are still using poisonous shit, and none of it is organic , even if the CBD is which I doubt(I am an organic cannabis farmer, and despise shit that's not organic trying to sound healthy). Start with bulk EtOH crude, clean it dewax it filter it, recover the solvent, and crash out the CBD, super simple as cbda will crash with no effort, and then you will be starting with a pure product
 
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