Síntese simples e crua de Δ8-THC sem solventes, perguntas

cvvvxa

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Olá, deparei-me com isto no youtube e queria partilhar e perguntar se alguém tem alguma experiência nisto, ou melhorias, uma vez que tenciono fazer em grande escala. O inglês não é a minha primeira língua, pelo que peço desculpa pelos erros
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Procedimento:
O CBD (25g) é misturado com P-TSA (0,5g) e colocado numa placa de aquecimento a 120C, agitado e aquecido durante uma hora. Depois disso, a mistura contém 75% de Delta 8 THC, 2,5% de Delta 9 THC, 4% de CBDA, 5% de exo-THC, 10% de iso-THC.

A minha questão principal é se seria possível fumar depois de lavar o ácido com água e base e se seria possível produzir Δ9 talvez aquecendo-o a 70C e mantendo-o lá durante mais tempo. Já vi métodos para obter Δ9, mas com solventes, e quero evitar isso porque é muito difícil livrar-me de litros de tolueno em comparação com isto. Também gostaria de saber se é possível remover a cor vermelha.
 

WillD

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É necessário utilizar o solvente. E outras condições com este reagente
 

mycelium

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There is a whole website devoted to cannabis extraction, which also includes a grip of CBD>D8 or d9.
PTSA is one way, I believe there is also a catalyst required.
I haven't been doing canna work for a few years and never did those reactions, but there are several paths that use different chemicals some make a lot of d8, some make a lot of d9, but ZERO people , and these are weed chemists a lot of them, have make d8 that does not have d9, and chromotography won't seperated them(what I read was a lot of solvent to seperated and the cost is crazy.

The d9 conversion is just as potent as distillate from weed, but it has a dif flavor(not that distillate has flavor, but yeah)
 

mycelium

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Further more, unless you have a grip of solventless CBD, then I don't know what you would start with solventless, because you are still using poisonous shit, and none of it is organic , even if the CBD is which I doubt(I am an organic cannabis farmer, and despise shit that's not organic trying to sound healthy). Start with bulk EtOH crude, clean it dewax it filter it, recover the solvent, and crash out the CBD, super simple as cbda will crash with no effort, and then you will be starting with a pure product
 
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