Paprasta neapdorota netirpinta Δ8-THC sintezė be tirpiklių, klausimai

[cvvvxa]

Sveiki, užtikau tai youtube ir norėjau pasidalyti bei paklausti, ar kas nors turi patirties šioje srityje, arba patobulinimų, nes planuoju gaminti dideliu mastu. Anglų kalba nėra mano gimtoji, todėl atsiprašau už klaidas
šaltinis :

Procedūra:
CBD (25 g) sumaišomas su P-TSA (0,5 g) ir dedamas ant kaitvietės, įkaitintos iki 120 C, maišomas ir kaitinamas valandą. Po to mišinyje yra 75 % Delta 8 THC, 2,5 % Delta 9 THC, 4 % CBDA, 5 % exo-THC, 10 % izo-THC.

Mano pagrindinis klausimas - ar būtų galima rūkyti nuplovus rūgštį vandeniu ir baze, ir ar Δ9 būtų galima pagaminti, galbūt kaitinant iki 70C ir ilgiau išlaikant. Jau mačiau Δ9 gamybos būdų, bet su tirpikliais, o aš noriu to išvengti, nes atsikratyti litrais tolueno yra kančia, palyginti su šiuo būdu. Be to, ar įmanoma pašalinti raudoną spalvą.

 

[WillD]

Jūs turite naudoti tirpiklį. Ir kitos sąlygos su šiuo reagentu

 

[mycelium]

There is a whole website devoted to cannabis extraction, which also includes a grip of CBD>D8 or d9.
PTSA is one way, I believe there is also a catalyst required.
I haven't been doing canna work for a few years and never did those reactions, but there are several paths that use different chemicals some make a lot of d8, some make a lot of d9, but ZERO people , and these are weed chemists a lot of them, have make d8 that does not have d9, and chromotography won't seperated them(what I read was a lot of solvent to seperated and the cost is crazy.

The d9 conversion is just as potent as distillate from weed, but it has a dif flavor(not that distillate has flavor, but yeah)

 

[mycelium]

Further more, unless you have a grip of solventless CBD, then I don't know what you would start with solventless, because you are still using poisonous shit, and none of it is organic , even if the CBD is which I doubt(I am an organic cannabis farmer, and despise shit that's not organic trying to sound healthy). Start with bulk EtOH crude, clean it dewax it filter it, recover the solvent, and crash out the CBD, super simple as cbda will crash with no effort, and then you will be starting with a pure product