Síntesis simple y cruda de Δ8-THC sin disolventes, preguntas

cvvvxa

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Hola me topé con esto en youtube y quería compartir y preguntar si alguien tiene alguna experiencia en esto, o mejoras ya que planeo hacer a gran escala. El inglés no es mi lengua materna así que perdón por los errores
fuente :

Procedimiento:
CBD(25g) se mezcla con P-TSA(0.5g) y se coloca en una placa caliente a 120C, se agita y se calienta durante una hora. Después la mezcla contiene 75% Delta 8 THC, 2.5% Delta 9 THC, 4% CBDA, 5% exo-THC, 10% iso-THC.

Mi pregunta principal es si sería fumable después de lavar el ácido con agua y base y si se podría producir Δ9 tal vez calentándolo a 70C y manteniéndolo allí durante más tiempo. Ya he visto métodos para Δ9 pero con disolventes y quiero evitar eso porque es un dolor para deshacerse de litros de tolueno en comparación con esto. También si podría ser posible quitar el color rojo.
 

WillD

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Debe utilizar el disolvente Y otras condiciones con este reactivo
 

mycelium

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There is a whole website devoted to cannabis extraction, which also includes a grip of CBD>D8 or d9.
PTSA is one way, I believe there is also a catalyst required.
I haven't been doing canna work for a few years and never did those reactions, but there are several paths that use different chemicals some make a lot of d8, some make a lot of d9, but ZERO people , and these are weed chemists a lot of them, have make d8 that does not have d9, and chromotography won't seperated them(what I read was a lot of solvent to seperated and the cost is crazy.

The d9 conversion is just as potent as distillate from weed, but it has a dif flavor(not that distillate has flavor, but yeah)
 

mycelium

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Further more, unless you have a grip of solventless CBD, then I don't know what you would start with solventless, because you are still using poisonous shit, and none of it is organic , even if the CBD is which I doubt(I am an organic cannabis farmer, and despise shit that's not organic trying to sound healthy). Start with bulk EtOH crude, clean it dewax it filter it, recover the solvent, and crash out the CBD, super simple as cbda will crash with no effort, and then you will be starting with a pure product
 
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