Shake and bake method for 4mmc

[kinshasa99]

Has anyone tryied shake and bake method for production of 4mmc with DCM?
Which are the risks involved?

 

[Netflix]

Yes you can use dcm toulen or benzen
You need to made
~2xJar
~1xTape
~2xPlastic Bag
~1xFunnel
~2xSyringe 100ml \ 50ml
~Old t~shirt

Whis is what you need form equipment

 

[Netflix]

Yes you can use dcm toulen or benzen
You need to made
~2xJar
~1xTape
~2xPlastic Bag
~1xFunnel
~2xSyringe 100ml \ 50ml
~Old t~shirt

Whis is what you need form

 

[The-Hive]

@fidelis found it

 

[Netflix]

Chemicals
{100g}
2-bromo-4methylopropiophenone
{500ml} dcm toulen or benzen
{200ml} methyloamine 40% in water
{3x300ml} cheap water from shop with no gas!!!
{500ml} acetone technical from the construction shop
{55ml} acid hcl 35%-38% if you have 31% acid then we need more to use
This all what we need to made this way

 

[ymaaah]

if I want to make a larger scale, like 1kg, I need to multipliate by 10 the reagents ect..?

 

[StarWars]

Yes

 

[ymaaah]

U said "cheap water from shop" but u dont need to use distillate water? Demineralized water can be good?

 

[41Dxflatline]

Drinking water is usually reverse osmosis and UV decontaminated.

 

[Netflix]

2-Bromo-4-methylpropiophenone in
DCM
Step 1

 

[WildDoc]

How much dcm for 1g od 2b4m?

 

[dr.zee]

300ml

 

[Benz88]

Why the bag? Can you explain more please

 

[Netflix]

to completely seal the jar. When I pour methylamine, the gas cannot escape, then in addition I seal the jar with the tape.

 

[antrax]

Is it more effective to close the container so that the gases from the methylamine 40% aqueous solution do not escape or leave the container open so that the gases escape freely?
Thank you!!

 

[Netflix]

Next step
Take
2-bromo-4methylopropiophenone 100g\50ml in dcm 500ml= 550ml
And monomethyloamine 40 in water 200ml
And take biger jar 750ml
drop 2b4m in dcm to big jar
and later monomethyloamine
use bag and tabe and shake 30 min

 

[Netflix]

You get 4mmc freebase in dcm on top you have monomethyloamine
You take out monomethyloamine and drop water and wash later we have
4mmc freebase oil

 

[Dexterror]

I have a question, why you takes the top part of the solution to heat it? the bottom part is 4mmc freebase? Then why you take top ?

 

[WildDoc]

Mmc freebase is on top or down?

 

[Netflix]

Freebase and water on top

 

[Netflix]

Later we use acid hcl 35%-38% 55ml and 500ml acetone
Drop 250ml acetone to oil and mix acid with acetone and all drop to freebase with acetone and fast mix wood and you wait 30min and you get ....4mmc hcl Ph 6\5.5

 

[Netflix]

Much people ask me how im get like this color oil simple if is pure 2b4m you get like this color oil
Next test

 

[Netflix]

When you drop to fast acid you born meph and is like this oil but
This time we get nice white milk

 

[ymaaah]

Hi Netflix

do you have a pdf synthesis of this?

 

[Methylamine]

Hi does anyone tryied this shake and bake method recipe?

 

[StarWars]

Video shake and bake

 

[HerrHaber]

A brief translation of what is going on in the video may help... it's just curiosity

 

[doctorpsi]

Please can you repost the video?

 

[doctorpsi]

it was deleted

 

[ymaaah]

whats the yield? Not a lot I imagine..?

 

[StarWars]

Made u will see

 

[StarWars]

Made u will see how much u get.

 

[ymaaah]

I will.