plz check the whole process and plz tell me which step i do mistake, mixture not perform white Flappy liquid.
20g 2b4m
100ml EA
stirrer until dissolve,
Then add 40ml MA 40%.
stirrer 1 hours temp not goes above 30.2. Without water bath.
then put in separating funnel.
first wash once with bicarbonate 5% 60 ml solution,
then 3 time wash with cold water 60ml x 3 times
After wash add 200ml chilled acetone.
Then dropping add hcl 33%.
After some add hcl color change yellow to brown.
Then
after some drop like 3-4 drop add hcl
change brown to green
after some time without dropping hcl color change to yellow.
But not performing white liquid.
As all saying
20g 2b4m
100ml EA
stirrer until dissolve,
Then add 40ml MA 40%.
stirrer 1 hours temp not goes above 30.2. Without water bath.
then put in separating funnel.
first wash once with bicarbonate 5% 60 ml solution,
then 3 time wash with cold water 60ml x 3 times
After wash add 200ml chilled acetone.
Then dropping add hcl 33%.
After some add hcl color change yellow to brown.
Then
after some drop like 3-4 drop add hcl
change brown to green
after some time without dropping hcl color change to yellow.
But not performing white liquid.
As all saying